Method of manufacturing a silica glass preform

• US 5,244,485 A
• Filed: 04/24/1992
• Issued: 09/14/1993
• Est. Priority Date: 04/30/1991
• Status: Expired due to Fees

• Current Assignee: Furukawa Electric Company Limited
• Original Assignee: Furukawa Electric Company Limited
• Inventors: Sato, Tsuguo, Hihara, Hiroshi, Enomoto, Noritsugu, Yagi, Takeshi, Yoshida, Kazuaki, Oku, Masato, Morikawa, Takayuki
• Primary Examiner(s): LINDSAY JR, ROBERT
• Application Number:
  US07/874,179
• Time in Patent Office: 508 Days
• Field of Search: 65/2, 65/3.11, 65/18.1, 65/18.3, 65/3.12
• US Class Current: 65/412
• CPC Class Codes: C03B 37/01282 by pressing or sintering, e.g. hot-pressing
• CPC Class Codes: Y02P 40/57 Improving the yield, e-g- reduction of reject rates

Abstract

The method of manufacturing a silica glass preform comprises the steps of inserting a rod-like member mainly containing a ductile material, into a forming space of a mold, charging the remaining space of the forming space with a forming material containing silica glass powder or doped silica glass powder, compressing the mold charged with the forming material from outside such as to form a porous glass body of the forming material around the rod-like member, removing the rod-like member from the porous glass body, inserting a glass rod into the hole formed after removal of the rod-like member, purifying said porous glass body in which the glass rod is inserted, and consolidating said porous glass body purified in the above purifying step.

Claims

1. A method of manufacturing a silica glass preform comprising the steps of:

inserting a rod-like member mainly containing a ductile material, into a forming space of a mold;

charging a remaining space of the forming space with a forming material containing silica glass powder, or doped silica glass powder;

compressing the mold charged with the forming material from outside such as to form a porous glass body of the forming material around the rod-like member;

removing the rod-like member from the porous glass body thereby forming a hole after removal of the rod-like member;

inserting a glass rod into the hole;

purifying said porous glass body in which the glass rod is inserted; and

consolidating said porous glass body purified in the above purifying step.

2. The method according to claim 1, wherein said removing step is performed after said purifying step.

3. The method according to claim 1, wherein said purifying step is performed between said removing step and said inserting step.

4. The method according to claim 1, wherein said rod-like member is formed mainly of a metal.

5. The method according to claim 4, wherein said rod-like member is formed of a metal coated with glass or synthetic resin on a surface thereof.

6. The method according to claim 1, wherein said forming material is silica powder, particles of which have an average diameter between a range of 0.4 to 25 μ

m.

7. The method according to claim 6, wherein said forming material contains 50% or more of granulated powder, grains of which have grain diameters between 30 μ

m and 300 μ

m, said granulated powder prepared from said silica powder.

8. The method according to claim 7, wherein said forming material contains 50% or more of granulated powder formed of grains having diameters of 30 μ

m or larger and 300 μ

m or less, and 1% or more and less than 10% of powder formed of grains having diameter of 10 μ

m or smaller.

9. The method according to claim 1, wherein said silica glass powder or doped silica glass powder contains powder originated from water glass.

10. The method according to claim 1, further comprising the step of removing static electricity from said forming material.

11. The method according to claim 10, further comprising the step of removing static electricity from said mold.

12. The method according to claim 1, wherein said forming material is moisturized before being filled into the forming space.

13. A method according to claim 12, wherein moisture of said forming material is equal to or more than 1 wt% and less than 5 wt%.

14. The method according to claim 1, wherein at least one of ends of the porous glass body is tapered into a conical shape or formed into a three-dimensional curved surface having a radius of curvature equal to or greater than an outside diameter of the porous glass body.

15. The method according to claim 1, wherein silica powder prepared by a chemical vapor deposition method such as flame hydrolysis reaction, oxidation reaction, paralysis reaction technique, or one obtained by processing the silica powder prepared, was used as silica glass powder.

16. The method according to claim 1, wherein silica powder prepared by oxidation of metal silicate, or one obtained by processing the silica powder, was used as silica glass powder.

17. The method according to claim 1, wherein at least one end of said rod like member projects out of said porous glass body.