Method and apparatus for dry particle analysis

• US 5,359,907 A
• Filed: 11/12/1992
• Issued: 11/01/1994
• Est. Priority Date: 11/12/1992
• Status: Expired due to Fees

• Current Assignee: Horiba Instruments Incorporated (Horiba Limited)
• Original Assignee: Horiba Instruments Incorporated (Horiba Limited)
• Inventors: Baker, Jeffrey P., Wright, Craig A., Mott, Steven C.
• Primary Examiner(s): Williams, Hezron E.
• Assistant Examiner(s): Dombroske, George M.
• Application Number:
  US07/975,019
• Time in Patent Office: 719 Days
• Field of Search: 356/335, 356/336, 356/438, 356/440, 73/865.5, 73/23.33, 73/23.41, 73/23.42, 73/24.03, 73/24.06, 73/864.81
• US Class Current: 73/865.5
• CPC Class Codes: G01N 15/0205 by optical means
• CPC Class Codes: G01N 15/1404 Handling flow, e.g. hydrodynamic focusing
• CPC Class Codes: G01N 21/85 Investigating moving fluids or granular solids

Abstract

A dry particle analyzer includes a vibrating sieve cup drizzling particles downwardly with first and second sheath air flows provided to separate the particles from boundary walls and to form the drizzling particles into a curtain for optical analysis. The particles drop vertically as a drizzle with gravitational assistance from a bulk sample to the analysis passage, after which their direction of movement is changed to horizontal and then upward for removal from the analyzer.

Claims

1. A dry particle analyzer comprising:

means for drizzling particles from a bulk sample thereof, means for providing a downward flow of first sheath ambient air around said drizzling particles, means for downwardly columnating the first sheath air flow and drizzling particles, means for providing a downward and columnar flow of second sheath ambient air around said columnated first sheath air and drizzled particles and substantially in velocity union therewith, and means defining a vertically downwardly extending optical analysis cell passage receiving the unified downward flow of drizzled particles and first and second sheath air for columnated downward flow therein, whereby the drizzled particles flow downwardly continuously from said bulk sample and through said analysis cell passage means.

2. The dry particle analyzer of claim 1 further including

exit passage means for receiving from said analysis cell passage means said downward flow of drizzled particles and sheath air flows and turning the combined flow through substantially 180 degrees for upward exit flow, whereby said analysis cell and exit passage means cooperatively define generally a J-shape.

3. The dry particle analyzer of claim 2 wherein said exit passage means defines a convergent-divergent venturi nozzle shape.

4. The dry particle analyzer of claim 3 wherein said exit passage means further includes a divergent pressure-recovery section leading to an exit port.

5. The dry particle analyzer of claim 4 including a housing member defining therein said analysis cell passage means and said exit passage means, said housing sealingly carrying opposed transparent windows bounding said analysis cell passage, and providing for optical interrogation of said drizzled particles.

6. The dry particle analyzer of claim 1 wherein said means for drizzling particles from a bulk sample thereof includes a sieve cup, and means for vibrating said sieve cup.

7. The dry particle analyzer of claim 6 wherein said means for vibrating said sieve cup includes means for imposing a vertical oscillation on said sieve cup.

8. The dry particle analyzer of claim 7 wherein said means for imposing said vertical oscillation on said sieve cup includes means for imposing a vertical orbital oscillation to said sieve cup.

9. The dry particle analyzer of claim 1 wherein said means for providing said first sheath air flow around said drizzling particles includes a conduit extending vertically downwardly from an upwardly open mouth and receiving therein a lower exit portion of said sieve cup, said lower exit portion of said sieve cup and said conduit mouth cooperating to define a first ambient air inlet circumscribing said sieve cup exit portion.

10. The dry particle analyzer of claim 9 wherein said means for downwardly columnating said first sheath air flow and drizzled particles includes said conduit including a convergent flow velocity-increasing section below said mouth thereof, and said convergent section blending smoothly into a cylindrical conduit section extending through said means for providing said second sheath air flow.

11. The dry particle analyzer of claim 10 wherein said means for providing said second sheath air flow includes a plenum chamber means around said conduit, said plenum chamber means defining an ambient air inlet and having a downwardly open air outlet through which extends said cylindrical conduit section, said plenum chamber means including at said air outlet thereof a cellular air flow guide surrounding said cylindrical conduit section.

12. The dry particle analyzer of claim 11 wherein said plenum chamber means further includes an air filter at said ambient air inlet.

13. The dry particle analyzer of claim 1 including means for delivering said drizzled particles as a curtain of downwardly flowing particles.

14. The dry particle analyzer of claim 13 including said means for providing said first sheath air including an elongate rectangular outlet out of which said drizzled particles and first sheath air flow.

15. A dry particle analyzer apparatus comprising drizzling means for dispersing particulates from a bulk sample thereof downwardly at a selected metered rate, a conduit defining an upwardly open mouth receiving the drizzling particles and a first vertically downward flow of ambient sheath air, said conduit directing said particulates and first sheath air still further downwardly along a convergent conduit section, thereby effecting an increase of flow velocity through an externally surrounding plenum of second sheath air, said surrounding plenum providing an inlet through which enters ambient air and said plenum channels air therein downwardly therefrom through a plenum exit including a multi-cellular flow-columnator around the conduit, said conduit includes an elongate cylindrical flow-columnating exit portion extending through the flow-columnator, and each of said conduit and said plenum with flow columnator has generally the same total air flow resistance to produce substantially the same air flow velocity for both the first and second sheath air flows to provide a homogeneous descending column of air which includes a centralized flow stream of air with the drizzle of particles at a known location in the air flow column, and disposed below the convergent conduit and second sheath air plenum and in sealed relation with the latter is a planar analysis cell defining an air flow path generally of J-shape, the analysis cell defines a vertically downwardly extending analysis passage having opposite transparent windows for passage of test radiation beams perpendicular to the plane of the J-shape, and below the analysis passage the analysis cell includes side walls defining a sub-critical convergent-divergent venturi nozzle shape which turns the air and particulate flow 180 degrees at the bottom of the J-shape and leads upwardly as a divergent pressure-recovery diffuser to an exit port.

16. The dry particle analyzer of claim 15 wherein said means for drizzling particles from a bulk sample thereof includes a sieve cup, and means for vibrating said sieve cup.

17. The dry particle analyzer of claim 16 wherein said means for vibrating said sieve cup includes means for imposing a vertical oscillation on said sieve cup.

18. The dry particle analyzer of claim 17 wherein said means for imposing said vertical oscillation on said sieve cup includes means for imposing a vertical orbital oscillation to said sieve cup.

19. The dry particle analyzer of claim 15 wherein said secondary sheath air plenum further includes an air filter at said inlet.

20. A method of dry particle analysis, said method including the steps of:

drizzling particles from a bulk sample thereof, providing a downward flow of first sheath ambient air around said drizzling particles, downwardly columnating the first sheath air flow and drizzling particles, providing a downward and columnar flow of second sheath ambient air around said columnated first sheath air and drizzled particles and substantially in velocity union therewith, uniting said first and said second air flows, defining a vertically downwardly extending optical analysis cell passage below and downwardly receiving the unified downward flow of drizzled particles and first and second sheath air flows for continued downward flow therein, and optically interrogating said drizzled particles in said analysis cell passage, whereby the drizzled particles flow continuously downwardly from said bulk sample and through said analysis cell passage.

21. The method of claim 20 further including the steps of flowing said unified flow of drizzled particles and first and second sheath air flows through a convergent-divergent venturi nozzle, and turning said unified flow substantially 180 degrees while traversing said venturi nozzle, to flow upwardly to an outlet port.