Reduction of discoloration in plastic materials

• US 5,622,259 A
• Filed: 06/07/1995
• Issued: 04/22/1997
• Est. Priority Date: 06/07/1995
• Status: Expired due to Fees

• Current Assignee: Medtronic Minimed Incorporated (Medtronic Plc)
• Original Assignee: Diametrics Medical Limited (Allegro Biodiesel Corp.)
• Inventors: Church, Jonathan M.
• Primary Examiner(s): Vargot, Mathieu D.
• Application Number:
  US08/473,681
• Time in Patent Office: 685 Days
• Field of Search: 264/488, 264/489, 264/494, 264/446, 264/232, 264/340, 264/1.38, 264/1.27, 425/174.4, 204/901, 206/363
• US Class Current: 206/363
• CPC Class Codes: A61L 2/08 Radiation
• CPC Class Codes: B29C 71/04 by wave energy or particle radiation , e.g. for curing or vulcanising preformed articles during moulding, e.g. in a mould B29C35/08
• CPC Class Codes: Y10S 204/901 Effecting a color change by wave energy

Abstract

A method for reducing discoloration in a discolored plastic material which has been subjected to sterilization by gamma radiation which includes exposing the plastic material to light having a wavelength within the range of 200 to 600 nm for a time sufficient to restore the original clarity. A sterilized pack for a medical device including plastic material in which the clarity has been restored by the method is also included.

Claims

1. A method for reducing discoloration in a discolored plastic material in which the discoloration was produced by sterilizing the plastic material with gamma radiation, which method comprises placing the material in a closed chamber containing at least one lamp which produces light having a wavelength within the range of 200 to 600 nm and exposing the material to said light for up to twenty four hours to reduce the discoloration in the plastic material until the material is substantially restored to its original appearance.

2. A method according to claim 1 in which the time of exposure is from twelve to twenty four hours.

3. A method according to claim 1, in which the source of light is one or more linear fluorescent lamps, each having a power of 120 watts and a narrow band emission peaking at a wavelength of about 420 nm with maximum output when the temperature of the coldest part of the lamp is about 40°

to 50°

C.

4. A method according to claim 3, in which the source of light is six to twelve of the said lamps mounted in an air-cooled cabinet having stainless steel walls.

5. A method according to claim 1, in which the plastic material is originally a clear transparent acrylic plastic material which has been discolored after being irradiated with gamma radiation and in which the original clarity is restored by subjecting the material to light having a peak wavelength maximum of 420 nm for a period of from twelve to twenty four hours.

6. A method according to claim 5, in which the material is in the form of a polymethyl methacrylate optical fibre.

7. A method according to claim 1, in which the plastic material is in the form of a container for a medical device at least one wall of which is made from a polycarbonate or clear transparent polyethylene terephthalate glycolate.

8. A sterilized pack for a medical device which comprises an envelope of transparent plastic material accommodating a device, at least part of which is made of plastic material, which pack has been sterilized by gamma radiation resulting in discoloration of at least some of the plastic material, wherein the original clarity of said plastic material is restored by exposing the pack to light having a wavelength within the range of 200 to 600 nm for a time up to twenty four hours to restore the original clarity.

9. A pack according to claim 8, in which the envelope is made from transparent polyethylene terephthalate glycolate and the device comprises at least one optical fiber made from polymethyl methacrylate.