Apparatus and method for affixing thin film material to sample cup used in X-ray spectroscopy

• US 6,009,766 A
• Filed: 09/02/1998
• Issued: 01/04/2000
• Est. Priority Date: 09/02/1998
• Status: Expired due to Term

• Current Assignee: Chemplex Industries, Inc.
• Original Assignee: Monte J. Solazzi
• Inventors: Solazzi, Monte J.
• Primary Examiner(s): Williams, Hezron
• Assistant Examiner(s): Tran, Thuy Vinh
• Application Number:
  US09/145,527
• Time in Patent Office: 489 Days
• Field of Search: 73/863, 73/866.5, 73/863.23, 73/864.91, 73/61.55, 356/246, 422/102, 378/208, 220/276
• US Class Current: 73/864.91
• CPC Class Codes: B01L 3/508 rigid containers not provided for above
• CPC Class Codes: G01N 23/2204 Specimen supports therefor; Sample conveying means therefore

Abstract

A method for covering a sample cup for retaining a sample to be analyzed spectrochemically, the method comprising the steps of attaching a thin-film material to a substrate having a through hole to form a planar frame member, the thin-film material covering the through hole and having a patterned perforation positioned within the through hole defining an inner covering surface with diameter d1 and an outer detaching surface; disposing the planar frame member onto an open top surface of the sample cup with diameter d2 less than d1 such that the inner covering surface of the thin-film material extends across the open top surface; and depressing a portion of the planar frame member to cause detachment of the thin-film material from the substrate along the patterned perforation, and thereby causing increased tautness of the inner covering surface which extends across the open top surface.

Claims

1. An apparatus for mounting a thin-film of material across an open end of a sample cup, said thin film for retaining a sample to be analyzed spectrochemically, said apparatus comprising:

a substrate having a through hole;

a thin film material bonded to said substrate and covering said through hole, said thin film material having a perforated line of weakness defining said thin film material into an inner region and an outer region, said line of weakness situated within said through hole;

wherein, application of said apparatus over an open end of a sample cup so that said inner region of said thin film material engages the sample cup and extends across the open end thereof causes said inner region to detach from said outer region of said thin film material thereby separating said apparatus from said inner region of said thin film material.

2. The apparatus according to claim 1, wherein said perforated line of weakness is circular.

3. The apparatus according to claim 1, wherein said through hole is circular.

4. The apparatus according to claim 1, wherein said substrate comprises a plastic.

5. The apparatus according to claim 1, wherein said substrate comprises a metal.

6. The apparatus according to claim 1, wherein said thin film material comprises polymide.

7. The apparatus according to claim 1, wherein said thin film material is selected from the group consisting of polyester, polymide, polycarbonate, and polypropylene.

8. The apparatus according to claim 1, wherein said thin film material is bonded to said substrate by ultrasonic bonding.

9. The apparatus according to claim 1, wherein said thin film material is bonded to said substrate by an adhesive.

10. A method for mounting a thin film of material across an open end of a sample cup used for retaining a sample to be analyzed spectrochemically, said method comprising the steps of:

providing a planar frame member having a through hole and a thin film material bonded thereto so that said thin film material covers said through hole, said thin film material having a perforated line of weakness positioned within said through hole, said perforated line of weakness defining said thin film material into an inner region and an outer region;

placing said planar frame member onto an open end of a sample cup of so that said inner region extends across said open end of said sample cup; and

simultaneously tautening said inner region of said thin film material and detaching said inner region of said thin film material from said outer region of said thin film material along said perforated line of weakness to separate said planar flame member from said sample cup.

11. The method according to claim 10, wherein said through hole is circular.

12. The method according to claim 10, wherein said planar frame member is selected from the group consisting of plastic, metal, and paper.

13. The method according to claim 10, wherein said thin film material is selected from the group consisting of polyester, polymide, polycarbonate, and polypropylene.

14. The method according to claim 10, wherein said perforated line of weakness is circular.

15. The method according to claim 10, wherein said simultaneous tautening and detaching step includes the steps of:

positioning a snap-on ring on said inner region of said thin film material;

depressing said snap-on ring to simultaneously tauten said inner region of said thin film material and detach said inner region of said thin film material from said outer region of said thin film material along said perforated line of weakness to separate said planar frame member from said sample cup.

16. The method according to claim 10, wherein said simultaneous tautening and detaching step includes the step of depressing a portion of said planar frame member to simultaneously tauten said inner region of said thin film material and detach said inner region of said thin film material from said outer region of said thin film material along said perforated line of weakness to separate said planar frame member from said sample cup.

17. The method according to claim 10, wherein said thin film material is adhesively bonded to said planar frame member.

18. The method according to claim 10, wherein said thin film material is ultrasonically bonded to said planar frame member.

19. An apparatus for mounting a thin film of material across an open end of a sample cup, said thin film for retaining a sample to be analyzed spectrochemically, said apparatus comprising:

a substrate having a through hole;

a thin film material bonded to said substrate and covering said through hole, said thin film material having a perforated line of weakness defining a thin film inner region situated within said through hole.

20. The apparatus according to claim 19, wherein said thin film material is selected from the group consisting of polyester, polymide, polycarbonate, and polypropylene.