Processing apparatus with an electromagnetic launch

• US 7,518,092 B2
• Filed: 03/15/2007
• Issued: 04/14/2009
• Est. Priority Date: 03/15/2007
• Status: Expired due to Fees

• Current Assignee: Capita Technologies Incorporated (The Interpublic Group of Companies, Inc.)
• Original Assignee: Capita Technologies Incorporated (The Interpublic Group of Companies, Inc.)
• Inventors: Purta, David A., Portnoff, Marc A.
• Primary Examiner(s): ROBINSON, DANIEL LEON
• Application Number:
  US11/686,586
• Publication Number:
  US 20080233020A1
• Time in Patent Office: 761 Days
• Field of Search: 219678-697, 422/21
• US Class Current: 219/695
• CPC Class Codes: B01J 19/126 Microwaves
• CPC Class Codes: B01J 2219/1215 Single reactor
• CPC Class Codes: B01J 2219/1227 Reactors comprising tubes with open ends
• CPC Class Codes: B01J 2219/1239 Means for feeding and evacuation
• CPC Class Codes: B01J 2219/1254 Static supports
• CPC Class Codes: B01J 2219/126 in the form of a closed housing
• CPC Class Codes: B01J 2219/1266 Microwave deflecting parts
• CPC Class Codes: B01J 2219/1269 Microwave guides
• CPC Class Codes: B01J 2219/1272 Materials of construction
• CPC Class Codes: B01J 2219/1296 Multiple sources
• CPC Class Codes: B01J 8/0257 in a cylindrical annular shaped bed

Abstract

A processing apparatus, such as a microwave-based processing apparatus. The apparatus includes a vessel having an inner surface defining a chamber configured to hold a reaction mixture, a guide, and a launch coupled to the guide. The guide can be at least partially disposed in the vessel, and is configured to propagate electromagnetic energy. The launch is configured to couple at least a portion of the electromagnetic energy from the guide to the reaction mixture. Example launches include a dielectric window and a projection. Example projections include a metallic projection and a dielectric projection.

Claims

1. A processing apparatus comprising:

a vessel including an inner surface defining a chamber configured to hold a reaction mixture, wherein the vessel further includes a port configured to introduce the reaction mixture, including at least one reactant and at least one catalyst, to the chamber and to release at least one product with or without the at least one catalyst from the chamber;

a guide including a first portion that extends into the chamber and is at least partially in contact with the reaction mixture, the guide being configured to propagate electromagnetic energy;

a first launch supported by the guide and disposed at least partially within the vessel, the first launch including a second portion that is in contact with the reaction mixture, the first launch being configured to launch a first portion of the electromagnetic energy from the guide into the reaction mixture; and

a second launch supported by the guide and including a third portion that extends into the chamber and that is in contact with the reaction mixture, the second launch configured to launch a second portion of the electromagnetic energy from the guide into the reaction mixture.

2. The apparatus of claim 1, wherein the vessel further includes a fixed bed to receive a heterogeneous catalyst.

3. The apparatus of claim 1, wherein the vessel includes an aperture, and the guide is at least partially disposed in the aperture.

4. The apparatus of claim 1, wherein the guide includes a dielectric-filled waveguide at least partially disposed within the vessel, and wherein the first launch is supported by the dielectric-filled waveguide.

5. The apparatus of claim 4, wherein the apparatus further comprises a radio frequency (RF) generator coupled to the dielectric-filled waveguide to propagate RF energy through the dielectric-filled waveguide.

6. The apparatus of claim 1, wherein the first launch includes a dielectric window.

7. The apparatus of claim 1, wherein the first launch includes a projection.

8. The apparatus of claim 7, wherein the projection includes a metallic projection.

9. The apparatus of claim 8, wherein the projection further includes a dielectric material at least partially surrounding the metallic projection.

10. The apparatus of claim 1, wherein the first launch includes a dielectric projection.

11. The apparatus of claim 10, wherein the first launch further includes a second dielectric material at least partially surrounding the dielectric projection.

12. The apparatus of claim 1, further comprising

a second guide including a fourth portion that extends into the chamber and is at least partially in contact with the reaction mixture, the second guide being configured to propagate electromagnetic energy;

and

wherein the second guide supports the second launch.

13. The apparatus of claim 1, wherein the first launch is integrally coupled with the guide.

14. The apparatus of claim 1, wherein the reaction mixture has a loss tangent, and wherein the first launch has a coupling efficiency into the reaction mixture, the coupling efficiency being greater than approximately 80 percent.

15. The apparatus of claim 14, wherein the coupling efficiency is greater than approximately 95 percent.

16. The apparatus of claim 14, wherein the loss tangent is less than 0.1.

45. The apparatus of claim 1, wherein the guide includes a second portion that extends into the chamber and is in contact with the reaction mixture.

17. A processing apparatus comprising:

a vessel including an inner surface defining a chamber configured to hold a reaction mixture, wherein the vessel further includes a port configured to introduce the reaction mixture, including at least one reactant and at least one catalyst to the chamber, and to release at least one product with or without the at least one catalyst from the chamber;

a guide configured to propagate electromagnetic energy; and

a first launch and a second launch coupled to the guide and including a respective portion that extends into the chamber and is in contact with the reaction mixture, each of the first launch and the second launch being configured to couple a portion of the electromagnetic energy from the guide into the reaction mixture.

18. The apparatus of claim 17, wherein the first launch includes a first metallic projection and the second launch includes a second metallic projection.

19. The apparatus of claim 18, wherein the guide includes a dielectric-filled waveguide, and wherein the first metallic projection and the second metallic projection are coupled to the dielectric-filled waveguide.

20. The apparatus of claim 19, wherein the apparatus further comprises a RF generator coupled to the dielectric-filled waveguide to propagate RF energy through the dielectric-filled waveguide.

21. The apparatus of claim 18, wherein the apparatus further comprises an electromagnetic generator, wherein the guide includes a first guide and a second guide coupled to the electromagnetic generator, and wherein the first guide includes the first metallic projection and the second guide includes the second metallic projection.

22. The apparatus of claim 21, wherein the electromagnetic generator includes a first electromagnetic generator coupled to the first guide and a second electromagnetic generator coupled to the second guide.

23. The apparatus of claim 18, wherein the apparatus further comprises an electromagnetic generator and a distributor coupled to the electromagnetic generator, wherein the guide includes a first guide and a second guide, wherein the first guide includes the first metallic projection and the second guide includes the second metallic projection.

25. The apparatus of claim 18, further comprising a dielectric material at least partially surrounding the first metallic projection.

26. The apparatus of claim 17, wherein the guide is disposed outside of the vessel.

27. The apparatus of claim 26, wherein the guide is at least partially disposed within the vessel.

24. A processing apparatus comprising:

a vessel including an inner surface defining a chamber configured to hold a reaction mixture;

a first guide configured to propagate electromagnetic energy;

a first metallic projection and a second metallic projection coupled to the first guide and including a respective portion that extends into the chamber and is in contact with the reaction mixture, each of the first metallic projection and the second metallic projection being configured to couple a portion of the electromagnetic energy from the first guide into the reaction mixture;

a second guide configured to propagate electromagnetic energy; and

a third metallic projection and a fourth metallic projection coupled to the second guide and including a respective portion that extends into the chamber and is in contact with the reaction mixture, each of the third metallic projection and the fourth metallic projection being configured to couple a portion of the electromagnetic energy from the second guide into the reaction mixture.

28. A processing apparatus comprising:

a vessel including an inner surface defining a chamber configured to hold a reaction mixture, wherein the vessel further includes a port configured to introduce the reaction mixture, including at least one reactant and at least one catalyst, to the chamber and to release at least one product with or without the at least one catalyst from the chamber;

a guide configured to propagate electromagnetic energy; and

a first dielectric projection and a second dielectric projection coupled to the guide and including a respective portion that extends into the chamber and is in contact with the reaction mixture, each of the first dielectric projection and the second dielectric projection being configured to couple a portion of the electromagnetic energy from the guide into the reaction mixture.

29. The apparatus of claim 28, wherein the guide includes a dielectric-filled waveguide, and wherein the first dielectric projection and the second dielectric projection are coupled to the dielectric-filled waveguide.

30. The apparatus of claim 29, wherein the apparatus further comprises a RF generator coupled to the dielectric-filled waveguide to propagate RF energy through the dielectric-filled waveguide.

31. The apparatus of claim 28, wherein the apparatus further comprises an electromagnetic generator, wherein the guide includes a first guide and a second guide coupled to the electromagnetic generator, wherein the first guide includes the first dielectric projection and the second guide includes the second dielectric projection.

32. The apparatus of claim 31, wherein the electromagnetic generator includes a first electromagnetic generator coupled to the first guide and a second electromagnetic generator coupled to the second guide.

33. The apparatus of claim 28, wherein the apparatus further comprises an electromagnetic generator and a distributor coupled to the electromagnetic generator, wherein the guide includes a first guide and a second guide, wherein the first guide includes the first dielectric projection and the second guide includes the second dielectric projection.

35. The apparatus of claim 28, wherein the guide is disposed outside of the vessel.

36. The apparatus of claim 28, wherein the guide is at least partially disposed within the vessel.

37. The apparatus of claim 28, further comprising a dielectric material at least partially surrounding the first dielectric projection.

34. A processing apparatus comprising:

a vessel including an inner surface defining a chamber configured to hold a reaction mixture;

a first guide configured to propagate electromagnetic energy;

a first dielectric projection and a second dielectric projection coupled to the guide and at least partially disposed within the vessel, each of the first dielectric projection and the second dielectric projection being configured to couple a portion of the electromagnetic energy from the guide into the reaction mixture;

a second guide configured to propagate electromagnetic energy; and

a third dielectric projection and a fourth dielectric projection coupled to the guide and at least partially disposed within the vessel, each of the third dielectric projection and the fourth dielectric projection being configured to couple a portion of the electromagnetic energy from the second guide into the reaction mixture.

38. The apparatus of claim 34, wherein the vessel further includes a port configured to introduce at least one reactant with or without at least one catalyst to the chamber and to release at least one product with or without at least one catalyst from the chamber.

39. The apparatus of claim 34, wherein the first guide and the second guide includes a first dielectric-filled waveguide and a second dielectric-filled wave guide, respectively, and wherein the first dielectric projection and the second dielectric projection are coupled to the first dielectric-filled waveguide, and the third dielectric projection and the fourth dielectric projection are coupled to the second dielectric-filled waveguide.

40. The apparatus of claim 34, wherein the electromagnetic generator includes a first electromagnetic generator coupled to the first guide and a second electromagnetic generator coupled to the second guide.

41. The apparatus of claim 34, wherein the apparatus further comprises an electromagnetic generator and a distributor coupled to the electromagnetic generator, wherein the first guide includes the first dielectric projection and the second guide includes the second dielectric projection.

42. The apparatus of claim 34, wherein the first guide and the second guide are disposed outside of the vessel.

43. The apparatus of claim 34, wherein the first guide is at least partially disposed within the vessel.

44. The apparatus of claim 34, wherein the first dielectric projection and the second dielectric projection are at least partially disposed into the chamber and in contact with the reaction mixture.