Method of processing ethanol byproducts and related subsystems

• US 7,601,858 B2
• Filed: 05/05/2005
• Issued: 10/13/2009
• Est. Priority Date: 08/17/2004
• Status: Active Grant

• Current Assignee: GS Cleantech Corporation (Greenshift Corporation)
• Original Assignee: GS Cleantech Corporation (Greenshift Corporation)
• Inventors: Cantrell, David Fred, Winsness, David J.
• Primary Examiner(s): Carr; Deborah D
• Application Number:
  US11/122,859
• Publication Number:
  US 20060041152A1
• Time in Patent Office: 1,622 Days
• Field of Search: 554/8
• US Class Current: 554/8
• CPC Class Codes: B01D 3/004 by continuous methods
• CPC Class Codes: C11B 1/00 Production of fats or fatty oils from raw materials
• CPC Class Codes: C11B 13/00 Recovery of fats, fatty oils or fatty acids from waste materials
• CPC Class Codes: C11B 3/001 by a combination of two or more of the means hereafter
• CPC Class Codes: C12F 3/10 from distillery slops
• CPC Class Codes: Y02W 30/74 Recovery of fats, fatty oils, fatty acids or other fatty substances, e.g. lanolin or waxes

Abstract

In one aspect of the invention, a method recovers oil from a concentrated byproduct, such as evaporated thin stillage formed during a dry milling process used for producing ethanol. The method includes forming a concentrate from the byproduct and recovering oil from the concentrate. The step of forming the concentrate may comprise evaporating the byproduct. Further, the step of separating the oil from the concentrate may comprise using a centrifuge and, in particular, a disk stack centrifuge. Other aspects of the invention include related methods and subsystems for recovering oil from thin stillage.

Claims

1. A method of recovering oil from thin stillage, the method comprising, in sequence:

evaporating the thin stillage to remove water and form a concentrated byproduct; and

recovering oil from the concentrated byproduct by heating and mechanically processing the concentrated byproduct to separate the oil from the concentrated byproduct, wherein the concentrated byproduct has a moisture content of greater than 30% and less than 90% by weight.

2. The method of claim 1, wherein the mechanical processing comprises separating the oil from the concentrated byproduct using a disk stack centrifuge.

3. The method of claim 1, wherein the recovering step is performed on the concentrated byproduct at a temperature of between about 150 and 212°

F.

4. The method of claim 1, wherein the recovering step is performed on the concentrated byproduct at a temperature of about 180°

F.

5. The method of claim 1, wherein the recovering step is performed on the concentrated byproduct having a pH of between about 3 and 6.

6. The method of claim 1, wherein the recovering step is performed on the concentrated byproduct having a pH of between about 3.5 and 4.5.

7. The method of claim 1, wherein the concentrated byproduct has a moisture content between about 60-85%.

8. A method of recovering oil from thin stillage, comprising, in sequence:

evaporating the thin stillage to create a concentrate having a moisture content of greater than 30% by weight and less than about 90% by weight; and

centrifuging the concentrate to recover oil.

9. The method according to claim 8, wherein the step of centrifuging the concentrate comprises using a disk stack centrifuge.

10. A method of processing whole stillage, comprising:

recovering thin stillage from the whole stillage, the thin stillage including oil and solids;

concentrating the thin stillage including the solids to produce a thin stillage concentrate, wherein the thin stillage concentrate has a moisture content of greater than 30% and less than 90% by weight; and

recovering oil from the concentrate by a process consisting essentially of heating and mechanically processing the concentrate to separate the oil from the concentrate.

11. The method of claim 10, wherein the step of recovering the thin stillage includes using a separator selected from the group consisting of a press, extruder, a decanter centrifuge, and a screen centrifuge.

12. The method of claim 10, wherein the concentrating step comprises processing the thin stillage to a temperature of between about 150 and 212°

F., a pH of between about 3 and 6.

13. The method of claim 10, wherein the step of recovering oil comprises separating the oil from the concentrate using a centrifuge.

14. The method of claim 10, wherein the recovering and concentrating steps are performed in a continuous fashion.

15. The method of claim 10, further including the step of drying the concentrate after the step of recovering the oil.

16. In a method for processing corn to produce ethanol and concentrated thin stillage, the improvement comprising the step of recovering a product consisting essentially of oil from the concentrated thin stillage by heating and mechanically processing the concentrated thin stillage to separate the oil from the concentrated thin stillage.