Method of processing ethanol byproducts and related subsystems

• US 8,008,516 B2
• Filed: 09/30/2005
• Issued: 08/30/2011
• Est. Priority Date: 08/17/2004
• Status: Active Grant

• Current Assignee: GS Cleantech Corporation (Greenshift Corporation)
• Original Assignee: GS Cleantech Corporation (Greenshift Corporation)
• Inventors: Cantrell, David Fred, Winsness, David J.
• Primary Examiner(s): Carr; Deborah D
• Application Number:
  US11/241,231
• Publication Number:
  US 20060041153A1
• Time in Patent Office: 2,160 Days
• Field of Search: 554/8
• US Class Current: 554/8
• CPC Class Codes: B01D 3/004 by continuous methods
• CPC Class Codes: C11B 1/00 Production of fats or fatty oils from raw materials
• CPC Class Codes: C11B 13/00 Recovery of fats, fatty oils or fatty acids from waste materials
• CPC Class Codes: C11B 3/001 by a combination of two or more of the means hereafter
• CPC Class Codes: C12F 3/10 from distillery slops
• CPC Class Codes: Y02W 30/74 Recovery of fats, fatty oils, fatty acids or other fatty substances, e.g. lanolin or waxes

Abstract

In one aspect of the invention, a method recovers oil from a concentrated byproduct, such as evaporated thin stillage formed during a dry milling process used for producing ethanol. The method includes forming a concentrate from the byproduct and recovering oil from the concentrate. The step of forming the concentrate may comprise evaporating the byproduct. Further, the step of separating the oil from the concentrate may comprise using a centrifuge and, in particular, a disk stack centrifuge. Other aspects of the invention include related methods and subsystems for recovering oil from thin stillage.

Claims

1. A method of recovering oil from thin stillage;

the method consisting essentially of, in sequence;

evaporating water from the thin stillage to form a thin stillage concentrate, wherein the thin stillage concentrate has a moisture content of greater than 30% and less than 90% by weight before the recovering step;

mechanically processing the thin stillage concentrate to separate oil from the thin stillage concentrate; and

recovering the separated oil.

2. The method of claim 1, wherein the thin stillage concentrate has a moisture content of greater than 60% and less than 85% by weight before the recovering step.

3. The method of claim 1, wherein the thin stillage concentrate has a pH of between about 3 and 6.

4. The method of claim 1, wherein the thin stillage concentrate has a pH of between about 3.5 and 4.5.

5. The method of claim 1, wherein mechanically processing further comprises heating the thin stillage concentrate to a temperature between 150°

F. and 212°

F.

6. The method of claim 1, wherein mechanically processing further comprises heating the thin stillage concentrate to a temperature between 150°

F. and 212°

F. and a pH between 3 and 6.

11. The method of recovering oil from thin stillage of claim 1, wherein mechanically processing comprises disc stack centrifuging the thin stillage concentrate.

7. A method of processing whole stillage, comprising, in sequence:

separating distiller wet grains and thin stillage from the whole stillage, the thin stillage including oil and solids;

concentrating the thin stillage including the solids to form a concentrate having a moisture content of greater than 30% and less than 90% by weight; and

disc stack centrifuging oil from the thin stillage concentrate to form a substantially oil free concentrate.

8. The method of claim 7, wherein the concentrating step comprises processing the thin stillage a pH of between about 3 and 6, and a moisture content of less than 90%.

9. The method of claim 7, wherein the recovering and concentrating steps are performed in a continuous fashion.

10. The method of claim 7, further including the step of drying the concentrate after the step of recovering the oil.