Calibration system, material delivery system, and methods for such delivery and calibration

• US 8,097,213 B2
• Filed: 10/24/2007
• Issued: 01/17/2012
• Est. Priority Date: 10/24/2007
• Status: Active Grant

• Current Assignee: Johnson Matthey Process Technologies Inc. (Johnson Matthey PLC)
• Original Assignee: Intercat Equipment, Inc.
• Inventors: Vierheilig, Al, Dorcheus, Brian
• Primary Examiner(s): Griffin, Walter
• Assistant Examiner(s): Seifu, Lessanework
• Application Number:
  US11/923,136
• Publication Number:
  US 20090110608A1
• Time in Patent Office: 1,546 Days
• Field of Search: 422/105, 422/107, 422/108, 422110-112, 422/232, 422/145, 73/11.3, 177/50
• US Class Current: 422/110
• CPC Class Codes: B01J 2208/00752 Feeding
• CPC Class Codes: B01J 8/0015 Feeding of the particles in the reactor; Evacuation of the particles out of the reactor
• CPC Class Codes: B01J 8/18 with fluidised particles combustion apparatus with fluidised bed in general F23C10/00; furnaces with fluidised bed F27B15/00
• CPC Class Codes: C10G 11/18 according to the "fluidised-bed" technique
• CPC Class Codes: C10G 50/00 Production of liquid hydrocarbon mixtures from lower carbon number hydrocarbons, e.g. by oligomerisation
• CPC Class Codes: G01G 13/00 Weighing apparatus with automatic feed or discharge for weighing-out batches of material for weighing a continuous stream G01G11/00; check-weighing G01G15/00; for fluids G01G17/04; apportioning by weight materials to be mixed G01G19/22; combinatorial weighing G01G19/387
• CPC Class Codes: G01G 23/3735 using a digital network

Abstract

Material delivery systems, methods of delivering material and methods of calibrating such systems and methods are disclosed. The material delivery system includes a delivery vessel, a load cell, and automated weight calibration device. The delivery vessel has at least an outlet adapted for coupling to an unit. The load cell is configured to provide a metric indicative of an amount of material in the delivery vessel. The automated weight calibration device is configured to impart a known force onto the at least one load cell. A method includes delivering material to a unit and determining how much material is delivered by a change in weight of a delivery vessel, wherein the delivery vessel comprises a load cell; applying a known calibration force to the load cell; and comparing a metric from the load cell of the known calibration with an expected metric.

Claims

1. A material delivery system comprising:

a delivery vessel adapted for coupling to an unit;

at least one load cell configured to provide a metric indicative of an amount of material in the delivery vessel; and

an automated load cell calibration device configured to impart a known force externally onto the delivery vessel and transmitted to the at least one load cell.

2. The material delivery system of claim 1, wherein the delivery vessel has at least an outlet adapted for coupling to an unit selected from a group consisting of a fluid catalyst cracking unit;

manufacture of pyridine and its derivatives, manufacture of polypropylene, manufacture of polyethylene, and manufacture of acrylonitrile.

3. The material delivery system of claim 1, wherein the automated load cell calibration device is adapted to impart a known force a plurality of times at desired frequency intervals.

4. The material delivery system of claim 1, wherein the automated load cell calibration device is adapted to directly or indirectly applying the known value onto the at least on load cells attach to the delivery vessel.

5. The material delivery system of claim 1, wherein the delivery vessel is a pressure vessel comprising a pressure control device coupled to the delivery vessel and configured to selectively pressurize the delivery vessel relative to at least one material storage container to a pressure sufficiently high enough to provide material to the unit.

6. The material delivery system of claim 1, further comprising a recording device to record the metric of the known force imparted on the vessel and determining any deviation between the recorded measured metric and known value of the force.

7. The material delivery system of claim 1, further comprising a feedback loop to take corrective action when the measured force deviates from the known value of desired force imparted by the calibration device.

8. The material delivery system of claim 1, wherein the automated load cell calibration device comprises physical calibration weight, pressure transmitter, electrical transducer, mechanical screw, and combinations thereof.

9. The material delivery system of claim 1, wherein the automated load cell calibration device comprises a pressure transmitter capable of imparting the known force directly without adding any material onto the vessel.

10. The material delivery system of claim 1, further comprising a plurality of separate material storage containers coupled to the vessel respectively via a plurality of inlets, a respective one of each inlet coupled to a separate material storage container.

11. The material delivery system of claim 10, wherein the at least one load cell is configured to provide a metric indicative of an amount of material dispensed from each separate material storage container.

12. The material delivery system of claim 10, further comprising a sensor to determine if the vessel is respectively coupled to the inlet of a material storage container from the plurality of separate material storage containers.

13. The material delivery system of claim 1, further comprising:

a separator disposed in the vessel and defining at least two compartments within the delivery vessel;

a plenum defined in the delivery vessel and fluidly coupled to each compartments; and

a plurality of outlets, a respective one of each outlets coupled to a respective compartment.

14. The material delivery system of claim 13, further comprising a sensor to determine if a specific hose is respectively coupled to an inlet of a compartment from plurality of compartments of the delivery vessel.

15. The material delivery system of claim 13, wherein the at least one load cell comprises a plurality of load cells, respectively one of each load cells coupled to a respective compartment to provide a metric indicative of an amount of material dispensed from each compartment of the delivery vessel to the unit.

16. A method of providing material to an unit comprising:

i) imparting a known force externally onto a delivery vessel and transmitting to at least a load cell coupled to the delivery vessel and measuring the known force imparted on the delivery vessel with a metric indicative of the known force, wherein the known force is imparted by providing the delivery vessel with a predetermined weight of material;

ii) calibrating the at least one load cell by comparing the known weight of material with the measured force; and

iii) delivering the material from the delivery vessel to the unit.

17. The method of claim 16, wherein the unit includes at least a unit selected from a group consisting of a fluid catalyst cracking unit;

manufacture of pyridine and its derivatives, manufacture of polypropylene, manufacture of polyethylene, and manufacture of acrylonitrile.

18. The method of claim 16, further comprising sending information concerning any deviation between the measured metric and known value of the force imparted by the calibration device to a remote control center outside of the unit.

19. The method of claim 16, further comprising recording the metric of the known force imparted on the delivery vessel and determining any deviation between the recorded measured metric and known value of the force.

20. The method of claim 16, further comprising performing any needed corrective action with respect to any deviation between the measured metric and known value of the force imparted by the calibration device.

21. A method comprising:

i) delivering material to an unit and determining how much material is delivered by a change in weight of a delivery vessel, wherein the delivery vessel comprises a load cell;

ii) applying a known calibration force externally onto the delivery vessel and transmitting to the load cell; and

iii) comparing a metric from the load cell of the known calibration force with an expected metric.

22. A method of automatically checking the calibration of a delivery vessel comprising:

i) placing a delivery vessel into a standby mode during which a material is not substantially added or removed from the delivery vessel, wherein the delivery vessel is coupled to at least a load cell;

ii) applying a known weight externally onto the delivery vessel, either directly or indirectly, and transmitting to the at least a load cell and measuring the applied weight while the delivery vessel is in the standby mode; and

iii) comparing the measured weight applied to the at least a load cell with the known weight to detect any deviation between the measured weight and known weight.

23. The method of claim 22, further comprising calibrating the vessel by making corrections to the actual weight of the delivery vessel based on the deviation between the known and measured weight.