Methods of processing ethanol byproducts and related subsystems

• US 8,283,484 B2
• Filed: 05/13/2011
• Issued: 10/09/2012
• Est. Priority Date: 08/17/2004
• Status: Active Grant

• Current Assignee: GS Cleantech Corporation (Greenshift Corporation)
• Original Assignee: GS Cleantech Corporation (Greenshift Corporation)
• Inventors: Cantrell, David Fred, Winsness, David J.
• Primary Examiner(s): Carr, Deborah D
• Application Number:
  US13/107,197
• Publication Number:
  US 20110282085A1
• Time in Patent Office: 515 Days
• Field of Search: 554/177
• US Class Current: 554/177
• CPC Class Codes: B01D 3/004 by continuous methods
• CPC Class Codes: C11B 1/00 Production of fats or fatty oils from raw materials
• CPC Class Codes: C11B 13/00 Recovery of fats, fatty oils or fatty acids from waste materials
• CPC Class Codes: C11B 3/001 by a combination of two or more of the means hereafter
• CPC Class Codes: C12F 3/10 from distillery slops
• CPC Class Codes: Y02W 30/74 Recovery of fats, fatty oils, fatty acids or other fatty substances, e.g. lanolin or waxes

Abstract

In one aspect of the invention, a method recovers oil from a concentrated byproduct, such as evaporated thin stillage formed during a dry milling process used for producing ethanol. The method includes forming a concentrate from the byproduct and recovering oil from the concentrate. The step of forming the concentrate may comprise evaporating the byproduct. Further, the step of separating the oil from the concentrate may comprise using a centrifuge and, in particular, a disk stack centrifuge. Other aspects of the invention include related methods and subsystems for recovering oil from thin stillage.

Claims

1. A method of recovering oil from thin stillage;

the method consisting essentially of, in sequence;

evaporating water from the thin stillage to form a thin stillage concentrate, wherein the thin stillage concentrate has a moisture content of greater than 30% and less than 90% by weight before the recovering step;

mechanically processing the thin stillage concentrate to separate oil from the thin stillage concentrate;

recovering the separated oil; and

drying the thin stillage concentrate to reduce the moisture content in the thin stillage concentrate.

2. The method of claim 1, wherein the mechanically processing the thin stillage concentrate to separate the oil from the thin stillage concentrate comprises introducing the thin stillage concentrate to a disk stack centrifuge.

3. The method of claim 1, wherein the recovering the oil is performed on the thin stillage concentrate at a temperature of between about 150 and 212°

F.

4. The method of claim 1, wherein the recovering the oil is performed on the thin stillage concentrate at a temperature of about 180°

F.

5. The method of claim 1, wherein the recovering the oil is performed on the thin stillage concentrate having a pH of between about 3 and 6.

6. The method of claim 1, wherein the recovering the oil is performed on the thin stillage concentrate having a pH of between about 3.5 and 4.5.

7. The method of claim 1, further comprising recovering an additional amount of oil from the thin stillage concentrate after drying the thin stillage concentrate.

26. The method of claim 1, wherein the drying of the thin stillage concentrate to reduce the moisture content in the thin stillage concentrate further comprises combining the thin stillage concentrate with wet distillers grains prior to the drying.

8. A method of processing whole stillage, comprising, in sequence:

separating distiller wet grains and thin stillage from the whole stillage, the thin stillage including oil and solids;

concentrating the thin stillage including the solids to form a thin stillage concentrate having a moisture content of greater than 30% and less than 90% by weight;

disc stack centrifuging oil from the thin stillage concentrate to form a substantially oil free concentrate; and

drying the thin stillage concentrate to reduce the moisture content in the thin stillage concentrate.

9. The method of claim 8, wherein the mechanically processing the thin stillage concentrate to separate the oil from the thin stillage concentrate comprises introducing the thin stillage concentrate to a disk stack centrifuge.

10. The method of claim 8, wherein the recovering the oil is performed on the thin stillage concentrate at a temperature of between about 150 and 212°

F.

11. The method of claim 8, wherein the recovering the oil is performed on the thin stillage concentrate at a temperature of about 180°

F.

12. The method of claim 8, wherein the recovering the oil is performed on the thin stillage concentrate having a pH of between about 3 and 6.

13. The method of claim 8, wherein the recovering the oil is performed on the thin stillage concentrate having a pH of between about 3.5 and 4.5.

14. The method of claim 8, wherein the thin stillage concentrate has a moisture content between about 60-85%.

15. The method of claim 8, further comprising recovering an additional amount of oil from the thin stillage concentrate after drying the thin stillage concentrate.

27. The method of claim 8, wherein the drying of the thin stillage concentrate to reduce the moisture content in the thin stillage concentrate further comprises combining the thin stillage concentrate with wet distillers grains prior to the drying.

16. A method of recovering oil from thin stillage, comprising, in sequence:

evaporating the thin stillage to create a thin stillage concentrate having a moisture content of greater than 30% by weight and less than about 90% by weight;

centrifuging the thin stillage concentrate to recover oil; and

drying the thin stillage concentrate to reduce a moisture content in the thin stillage concentrate.

17. The method according to claim 16, wherein the step of centrifuging the concentrate comprises using a disk stack centrifuge.

18. The method of claim 16, further comprising recovering an additional amount of oil from the thin stillage concentrate after drying the thin stillage concentrate.

28. The method of claim 16, wherein the drying of the thin stillage concentrate to reduce the moisture content in the thin stillage concentrate further comprises combining the thin stillage concentrate with wet distillers grains prior to the drying.

19. A method of recovering oil from thin stillage, the method comprising, in sequence:

evaporating the thin stillage to remove water and form a concentrated byproduct, wherein the concentrated byproduct has a moisture content of greater than 30% and less than 90% by weight;

recovering oil from the concentrated byproduct by heating and mechanically processing the concentrated byproduct to separate the oil from the concentrated byproduct; and

drying the concentrated byproduct to reduce the moisture content in the concentrated byproduct.

20. The method of claim 19, wherein the mechanically processing the thin stillage concentrate to separate the oil from the concentrated byproduct comprises introducing the thin stillage concentrate to a disk stack centrifuge.

21. The method of claim 19, wherein the recovering the oil is performed on the thin stillage concentrate at a temperature of between about 150 and 212°

F.

22. The method of claim 19, wherein the recovering the oil is performed on the thin stillage concentrate at a temperature of about 180°

F.

23. The method of claim 19, wherein the recovering the oil is performed on the thin stillage concentrate having a pH of between about 3 and 6.

24. The method of claim 19, wherein the recovering the oil is performed on the thin stillage concentrate having a pH of between about 3.5 and 4.5.

25. The method of claim 19, further comprising recovering an additional amount of oil from the thin stillage concentrate after drying the thin stillage concentrate.

29. The method of claim 19, drying the concentrated byproduct to reduce the moisture content in the concentrated byproduct further comprises combining the concentrated byproduct with wet distillers grains prior to the drying.

30. A method of recovering oil from thin stillage;

the method comprising

evaporating water from the thin stillage to form a thin stillage concentrate, wherein the thin stillage concentrate has a moisture content of greater than 30% and less than 90% by weight;

mechanically processing the thin stillage concentrate to separate oil from the thin stillage concentrate; and

recovering the separated oil.