Polycrystalline diamond cutting elements with engineered porosity and method for manufacturing such cutting elements

• US 8,783,389 B2
• Filed: 06/18/2010
• Issued: 07/22/2014
• Est. Priority Date: 06/18/2009
• Status: Active Grant

• Current Assignee: Smith International Incorporated (Schlumberger NV)
• Original Assignee: Smith International Incorporated (Schlumberger NV)
• Inventors: Fan, Guojiang, Yu, Feng, Fang, Yi, Belnap, J. Daniel, Cariveau, Peter T.
• Primary Examiner(s): HUTCHINS, CATHLEEN R
• Application Number:
  US12/818,780
• Publication Number:
  US 20100320006A1
• Time in Patent Office: 1,495 Days
• Field of Search: 175/420.2, 175/433, 175/434, 175/405.1, 512/96
• US Class Current: 175/433
• CPC Class Codes: B24D 18/0009 using moulds or presses
• CPC Class Codes: B24D 18/0027 by impregnation
• CPC Class Codes: B24D 99/005 Segments of abrasive wheels
• CPC Class Codes: C23F 1/02 Local etching
• CPC Class Codes: C23F 1/28 for etching iron group metals
• CPC Class Codes: E21B 10/36 Percussion drill bits with helical conveying portion E21B10/445; characterised by wear resisting parts E21B10/46
• CPC Class Codes: E21B 10/55 with preformed cutting elements
• CPC Class Codes: E21B 10/567 with preformed cutting elements mounted on a distinct support, e.g. polycrystalline inserts

Abstract

A method for facilitating infiltration of an infiltrant material into a TSP material during re-bonding of the TSP material to a substrate, by enhancing the porosity of the TSP material near the interface with the substrate is provided. Cutting elements formed by such method and downhole tools including such cutting elements are also provided.

Claims

1. A cutting element comprising:

a substrate; and

a preformed thermally stable polycrystalline diamond body bonded to the substrate with at least an infiltrant,

wherein the thermally stable polycrystalline diamond body comprises;

a working surface opposite the substrate;

a material microstructure comprising a plurality of bonded-together diamond crystals, and pores between the diamond crystals, the pores being substantially free of a catalyst material;

a first portion of the material microstructure proximate the substrate and having a porosity; and

a second portion of the material microstructure adjacent said first portion along an interface and extending to at least proximate the working surface and having a porosity,

wherein the first portion occupies at least 25% of a volume of the polycrystalline diamond body,

wherein the first portion comprises said infiltrant material in one or more of the pores between the diamond crystals previously occupied by a catalyst and a filler, said filler being different from said catalyst, and

wherein the material microstructure has a differential porosity of at least 1.6% between the first and second portions when said porosities are measured without said infiltrant.

2. The cutting element of claim 1, wherein the first portion comprises a first layer of the polycrystalline diamond body and the second portion comprises a second layer of the polycrystalline diamond body, and wherein the first and second layers meet along said interface.

3. The cutting element of claim 2, wherein the interface is domed.

4. The cutting element of claim 3 wherein thermally stable polycrystalline diamond body comprises a peripheral surface extending from the substrate to the working surface, wherein an edge is defined at an intersection of the peripheral surface and the working surface.

5. The cutting element of claim 4 wherein the working surface is flat.

6. The cutting element of claim 2, wherein the interface is planar.

7. The cutting element as recited in claim 2, wherein the second layer comprises a depression and wherein the first layer comprises a projection received within said depression.

8. The cutting element of claim 7, wherein the depression is complementary to said projection.

9. The cutting element of claim 7, wherein the projection is domed shaped.

10. A downhole tool comprising a tool body and at least one cutting element as claimed in claim 7 disposed thereon.

11. The downhole tool of claim 10, wherein the downhole tool comprises a drill bit.

12. The cutting element of claim 1, wherein the differential porosity is at least 2.6%.

13. The cutting element of claim 1, wherein the differential porosity is at least 3.4%.

14. The cutting element of claim 1, wherein one or more pores in the first portion comprise a trace amount of the filler material, the filler material being selected from the group consisting of tungsten carbide, silicone carbide, and metals not in Group VIII of the Periodic Table.

15. The cutting element of claim 14, wherein the filler material is tungsten carbide.

16. The cutting element of claim 1, wherein the second portion comprises the infiltrant material in one or more of the pores between the diamond crystals.

17. The cutting element of claim 16, wherein the working surface comprises the infiltrant material in one or more of the pores between the diamond crystals.

18. The cutting element of claim 1, wherein the first portion comprises a first layer and the second portion comprises a second layer, and wherein the first and second layers are each approximately 50% of the volume of the polycrystalline diamond body.

19. A downhole tool comprising a tool body and at least one cutting element as claimed in claim 1 disposed thereon.

20. The downhole tool of claim 19, wherein the downhole tool comprises a drill bit.

21. The cutting element of claim 1 wherein the porosity of the first portion is greater than the porosity of the second portion, wherein the porosity of the material microstructure is decreased by at least 1.6% across the interface from the first to the second portion.

22. The cutting element of claim 1, wherein the diamond crystals of said first portion have a first average grain size and wherein the diamond crystals of second portion have a second average grain size that is the same and the first average grain size.

23. The cutting element as recited in claim 1, wherein the diamond crystals of said first portion have a first grain size distribution and wherein the diamond crystals of second portion have a second grain size distribution that is the same and the first grain size distribution.

24. A cutting element comprising:

a substrate; and

a preformed thermally stable polycrystalline diamond body bonded to the substrate with at least an infiltrant,

wherein the thermally stable polycrystalline diamond body comprises;

a working surface opposite the substrate;

a peripheral surface extending from the substrate to the working surface, wherein an edge is defined at an intersection of the peripheral surface and the working surface;

a material microstructure comprising a plurality of bonded-together diamond crystals, and pores between the diamond crystals, the pores being substantially free of a catalyst material;

a first portion of the material microstructure proximate the substrate having a porosity and comprising a projection; and

a second portion of the material microstructure extending to at least proximate the working surface having a porosity and comprising a depression receiving said projection,

wherein the first portion comprises said infiltrant material in one or more of the pores between the diamond crystals previously occupied by a catalyst and a filler, said filler being different from said catalyst, and

wherein the material microstructure has a differential porosity between the first and second portions when said porosities are measured without said infiltrant.

25. The cutting element of claim 24 wherein the porosity of the first portion is greater than the porosity of the second portion, wherein the porosity of the material microstructure is decreased by at least 1.6% across the interface from the first to the second portion.

26. A downhole tool comprising a tool body and at least one cutting element as claimed in claim 24 disposed thereon.

27. The downhole tool of claim 26, wherein the downhole tool comprises a drill bit.

28. The cutting element of claim 24, wherein the diamond crystals of said first portion have a first average grain size and wherein the diamond crystals of second portion have a second average grain size that is the same and the first average grain size.

29. The cutting element as recited in claim 24, wherein the diamond crystals of said first portion have a first grain size distribution and wherein the diamond crystals of second portion have a second grain size distribution that is the same and the first grain size distribution.

30. A cutting element comprising:

a substrate; and

a preformed thermally stable polycrystalline diamond body bonded to the substrate with at least an infiltrant,

wherein the thermally stable polycrystalline diamond body comprises;

a working surface opposite the substrate;

a material microstructure comprising a plurality of bonded-together diamond crystals, and pores between the diamond crystals, the pores being substantially free of a catalyst material;

a first portion of the material microstructure proximate the substrate and having a porosity; and

a second portion of the material microstructure adjacent said first portion along an interface and extending to at least proximate the working surface and having a porosity,

wherein the first portion occupies at least 25% of a volume of the polycrystalline diamond body,

wherein the first portion comprises said infiltrant material in one or more of the pores between the diamond crystals previously occupied by a catalyst and a filler, said filler being different from said catalyst,

wherein the diamond crystals of said first portion have a first average grain size and the diamond crystals of the second portion have a second average grain size that is the same as the first average grain size, and

wherein the material microstructure has a differential porosity of at least 1.6% between the first and second portions when said porosities are measured without said infiltrant.

31. The cutting element of claim 30, wherein the first portion comprises a first layer of the polycrystalline diamond body and the second portion comprises a second layer of the polycrystalline diamond body, and wherein the first and second layers meet along said interface.

32. The cutting element of claim 30, wherein the interface is domed.

33. The cutting element of claim 30, wherein the interface is planar.

34. The cutting element as recited in claim 30, wherein the second layer comprises a depression and wherein the first layer comprises a projection received within said depression.