Chemical synthesis method of 10-methoxyl-5H-dibenz[b,f]azapine

Chemical synthesis method of 10-methoxyl-5H-dibenz[b,f]azapine

  • CN 101,386,595 B
  • Filed: 10/28/2008
  • Issued: 05/23/2012
  • Est. Priority Date: 10/28/2008
  • Status: Active Grant
First Claim
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1. the chemical synthesis process of 10-methoxyl group-5H-dibenzo [b, f] azatropylidene is characterized in that, adopts 10;

  • 11-dibromo iminodibenzyl is a raw material, reacts in methyl alcohol with Pottasium Hydroxide or potassium methylate to generate said 10-methoxyl group-5H-dibenzo [b, f] azatropylidene, steams methyl alcohol through decompression;

    Add water and stir, filtration drying, thus obtain 10-methoxyl group-5H-dibenzo [b, f] azatropylidene bullion;

    In said 10-methoxyl group-5H-dibenzo [b, f] azatropylidene bullion, add the dissolving of solvent post-heating, cooling, crystallization;

    Filtration drying, thus 10-methoxyl group-5H-dibenzo [b, f] azatropylidene elaboration obtained.

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