The manufacture method of organic alkali metal compound and organo-transition metal compound

The manufacture method of organic alkali metal compound and organo-transition metal compound

  • CN 101,874,033 B
  • Filed: 12/02/2008
  • Issued: 05/11/2016
  • Est. Priority Date: 12/04/2007
  • Status: Active Grant
First Claim
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1. the manufacture method of organo-transition metal compound being represented by following general formula (6), is characterized in that, by followingWhat general formula (1) represented have methine hydrogen or methylene hydrogen as active proton containing active proton compound and alkali metalIn the reaction of compound, add the olefin(e) compound being represented by following general formula (2), obtain the organic base gold that following general formula (3) representsBelong to compound, and in described reaction, use as solvent hydro carbons and aliphatic ethers, hydro carbons and aliphatic ethersMixed volume, than being in hydro carbons/aliphatic ethers scope that is 95/5~

  • 85/15, makes the described organic alkali metal compound obtainingReact with the transistion metal compound being represented by following general formula (5),RHp

    (1)In general formula (1), R represents alkyl or amino, also can contain halogen atom, silicon atom, oxygen atom or nitrogen-atoms;

    H tableShow the active proton of methine hydrogen or methylene hydrogen;

    P be with the number of hydrogen atoms being removed in the reacting of alkali metal compound,

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