Process for preparing metal hydroxides, hydroxyl organometals and white carbon suitable for use in ayurvedic medicine

Process for preparing metal hydroxides, hydroxyl organometals and white carbon suitable for use in ayurvedic medicine

  • CN 102,481,314 A
  • Filed: 08/13/2010
  • Published: 05/30/2012
  • Est. Priority Date: 08/13/2009
  • Status: Active Application
First Claim
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1. method for preparing metal hydroxides, hydroxyl organo-metallic compound and white carbon said method comprising the steps of:

  • I) carbon and/or at least a metal are provided;

    II) make said carbon and/or at least a metal 15% to 25%H 2O 2Acid solution in experience electrolysis, continue 24 to 72 hours time period;

    III) make from Step II) processing of the mixture that obtains experience period 1, comprising;

    A) adding other 20% to 30%H 2O 2Acid solution after, made this mixture sedimentation about 48 hours, stirred this mixture in per approximately simultaneously 12 hours;

    B) through making the microwave radiation of the mixture experience 200-270W power that obtains from step a), this mixture is concentrated to about 20% of its volume;

    C) recover volume and stirring through adding infiltration water;

    D) repeating step b)-c) 3 times, repeating step b then);

    IV) make the processing of the spissated mixture experience second round that obtains from step d), comprising;

    E) add 30% to 40%H 2O 2Acid solution with infiltration water;

    F) through making the microwave radiation of the mixture experience 400-450W power that obtains from step f), this mixture is concentrated to about 5%-10% of its volume;

    G) recover volume and stirring through adding infiltration water;

    H) repeating step f)-g) 4 times, repeating step f then);

    V) make from step h) processing of spissated mixture experience period 3 of obtaining, comprising;

    I) add 40% to 50%H 2O 2Acid solution with infiltration water;

    L) through making from step I) microwave radiation of the mixture that obtains experience 600-650W power, dry this mixture;

    M) recover volume and stirring through adding infiltration water;

    N) repeating step l)-m) 3 times, repeating step l then);

    VI) make from step n) processing of spissated mixture experience period 4 of obtaining, comprising;

    O) add 20%H 2O 2Acid solution with infiltration water;

    P) through making from step o) microwave radiation of the mixture that obtains experience 700-850W power, dry this mixture;

    Q) recover volume and stirring through adding infiltration water;

    R) repeating step p)-q) 3 times, repeating step p then);

    VII) make from step r) processing of spissated mixture experience period 5 of obtaining, comprising;

    S) add infiltration water;

    T) through making from step s) microwave radiation of the mixture that obtains experience 1000-3000W power, dry this mixture;

    U) recover volume and stirring through adding infiltration water;

    V) repeating step t)-u) 6 time.

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