A kind of method preparing high water solubility fullerol

A kind of method preparing high water solubility fullerol

  • CN 102,583,303 B
  • Filed: 02/24/2012
  • Issued: 12/09/2015
  • Est. Priority Date: 02/24/2012
  • Status: Active Grant
First Claim
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1. prepare the method that richness strangles alcohol, comprise the steps:

  • 1) oxide treatment is carried out to soccerballene, obtain fullerene peroxide;

    2) described fullerene peroxide and the hydroxylating agent with oxidisability are reacted, obtain richness and strangle alcohol;

    Step

         1) in oxide treatment carried out to soccerballene method be Ozonation;

    The gas adopted in described Ozonation is O 3or O 3and O 2mixed gas, O in described mixed gas 3volumn concentration be 0.1% ~ 100%;

    Step

         2) described in there is oxidisability hydroxylating agent be H 2o 2;

    Step

         2) described in reaction temperature of reaction be 30 DEG C-120 DEG C;

    The described reaction times is no less than 1 hour.

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