A kind of preparation method of nitrating Graphene

A kind of preparation method of nitrating Graphene

CN
  • CN 102,887,501 B
  • Filed: 07/21/2011
  • Issued: 02/03/2016
  • Est. Priority Date: 07/21/2011
  • Status: Active Grant
First Claim
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1. a preparation method for nitrating Graphene, comprises the steps:

  • Substrate, solid-state and/or liquid organic carbon source compound and solid-state and/or liquid organic nitrogen source compounds are provided;

    Wherein, described organic carbon source compound is at least one in dicyclopentadienylcobalt, nickelocene, two luxuriant manganese;

    Described organic nitrogen source compounds is at least one in urea, aniline, N-methyl-p-nitroaniline;

    The carbon and nitrogen atoms mol ratio of described organic carbon source compound and organic nitrogen source compounds is 2 ~ 20;

    1;

    By described organic carbon source compound and organic nitrogen source compounds mixing, and be mixed with mixture solution or suspension liquid;

    Described mixture solution or suspension liquid are coated in described substrate surface;

    10 are less than in oxygen-free environment, vacuum tightness -3under the vacuum condition of Pa, the described substrate being coated with mixture solution or suspension liquid is warming up to 500 ~ 1300 DEG C and makes mixture reaction 1 ~ 300 minute, generate described nitrating Graphene;

    Catalyzer is not added in the preparation method of described nitrating Graphene.

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