With the preparation method for promoting the Chinese traditional compound medicine slept of calming the nerves

With the preparation method for promoting the Chinese traditional compound medicine slept of calming the nerves

  • CN 103,860,872 B
  • Filed: 03/25/2014
  • Issued: 07/19/2019
  • Est. Priority Date: 03/25/2014
  • Status: Active Grant
First Claim
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1. Promote the preparation method for the Chinese traditional compound medicine slept 1. calming the nerves, includes the following steps:

  • (1) it stocks up;

    Take radish seed 30kg, Radix Angelicae Sinensis 18kg, Radix Astragali 22kg, cassia seed 38kg, Radix Ophiopogonis 18kg;

    Dried immature fruit of citron orange 12kg;

    (2) radish seed and cassia seed powder are broken into 14 mesh coarse powder, use titanium dioxide under the conditions of 35 DEG C, pressure 18MPa with Radix Angelicae SinensisCarbon supercritical methanol technology is extracted, and is collected and is extracted functional component, and the dregs of a decoction after extracting functional component are spare;

    (3) step (2) are extracted to the dregs of a decoction and Radix Astragali, Radix Ophiopogonis and the dried immature fruit of citron orange after functional component, it is small that the decoction 2.5 of 1000kg water is addedWhen, filtering obtains first time filtrate;

    The water that obtained filter residue adds 550kg decocts 0.8 hour, and filtering obtains second of filterLiquid;

    Merge first time filtrate and second of filtrate, is concentrated under reduced pressure under the conditions of 90 DEG C of Yu Wendu, vacuum degree -0.03MPa relatively closeDegree is 1.09, obtains concentrated extract, which is centrifuged using supercentrifuge, the parameter of centrifuge are as follows;

    flow velocity 2.8L/Min, revolving speed 16000r/min obtain concentration clear liquid;

    (4) the concentration clear liquid for obtaining means of supercritical extraction functional component that step (2) obtains, step (3), adds the oligomeric of 50kgWood molasses, purified water are configured to 250L oral solution, boiling sterilization 30 minutes, filling, and qualification is examined to obtain oral solution 12120.

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