Preparation method for polymer carbon material

Preparation method for polymer carbon material

  • CN 104,086,678 A
  • Filed: 07/17/2014
  • Published: 10/08/2014
  • Est. Priority Date: 07/17/2014
  • Status: Active Application
First Claim
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1. the preparation method of a polymkeric substance carbon material, this preparation method characteristic is taking active basic metal or alkaline-earth metal and polyalkenyl halides, halogenated polyolefin, polyhalohydrocarbon or derivatives thereof as raw material, metal linked reaction by halohydrocarbon is prepared high quality polymer carbon material, comprises the following steps:

  • (1) under protection of inert gas, active basic metal or alkaline-earth metal are dispersed in the body of polyalkenyl halides, halogenated polyolefin, polyhalohydrocarbon or derivatives thereof or its solution and carry out linked reaction, or the body of polyalkenyl halides, halogenated polyolefin, polyhalohydrocarbon or derivatives thereof or its solution are dripped or added in active basic metal and alkaline-earth metal reaction system, in encloses container under 0-300 °

    of C, carry out, after linked reaction 0.1-72 hour, making the suspension of polymkeric substance carbon material;

    (2) in the suspension of above-mentioned polymkeric substance, adding halogen, alcohol, water or acid to remove active basic metal or alkaline-earth metal makes and contains halogen or the polymkeric substance carbon material of halogen-containing replacement not;

    (3) after this mixture is filtered, then carry out being repeatedly dried after organic solvent washing, pickling (or alkali cleaning), washing, filtration, remove solvent and by product in carbon material aaerosol solution, make polymkeric substance carbon material.

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