Novel organic titanate butanediol titanium, and synthesis method and application thereof

Novel organic titanate butanediol titanium, and synthesis method and application thereof

  • CN 105,646,570 A
  • Filed: 01/11/2016
  • Published: 06/08/2016
  • Est. Priority Date: 11/06/2015
  • Status: Active Application
First Claim
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1. the synthetic method of a novel organotitanium acid esters butanediol titanium, it is characterised in that comprise the steps:

  • 1) solid sodium hydroxide or potassium hydroxide are dissolved in excessive BDO, then remove the water that reaction generates under reduced pressure, it is thus achieved that the sodium alkoxide of BDO or potassium alkoxide solution;

    2) under atmosphere of inert gases, titanium tetrachloride is dropped in step

         1) products therefrom, dropwise, stand, make sodium chloride or the potassium chloride salt crystalline deposit of generation;

    3) solid-liquid separation, obtains the BDO solution of the butanediol titanium of yellow transparent, removes BDO under reduced pressure, obtain white solid, is target product butanediol titanium.

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