Amine synthetic method

Amine synthetic method

  • CN 1,552,728 B
  • Filed: 05/29/2003
  • Issued: 04/18/2012
  • Est. Priority Date: 05/29/2003
  • Status: Active Grant
First Claim
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1. the compound method of a Somatostatin is characterized in that, this method comprises the following steps:

  • (1) be starting raw material with the Wang resin, the amino acid of protecting with Fmoc is monomer, connects amino acid one by one;

    (2) cut peptide with cutting peptide reagent, add the thick peptide of ether sedimentation;

    (3) at pH7.0-10.0, under 15-35 ℃

    , the blowing air oxidation;

    (4) carry out separation and purification with the C18 post.

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